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• W2053193516 abstract "Abstract The grinding of a 2: 1 molar ratio mixture of isonitrosoacetylacetone and 1,3-diaminopropan-2-ol led to formation of the tribasic ligand (H3L), (1) with two oxime groups and a flexible alcoholic backbone. The 1:2 molar ratio reaction of (1) with CuX2 produced the planar dinuclear complexes LCu2(X) nH2O; × = acetate (2), phenylacetate (3), formate (4), monochloroacetate (5), dichloroacetate (6), trichloroacetate (7), benzoate (8), and p-hydroxybenzoate (9); n = 1 for (2) and (8); n = 2 for (3)-(7); and n = 4 for (9). The copper(II) ions are bridged by the carbox-ylate and the alcoholic oxygen. The strong antiferromagnetic interactions in (2)-(9) are impeded in (5)-(7) by the chloroacetate bridge withdrawing electron density from the carboxylate. The latter bridge is replaced by picrate in the 1:1 molar ratio reaction of (2) with picric acid (10). The 1:1 molar ratio reaction of (1) with copper(II) acetate produced the tetranuclear [HLCu]2[LCu2(OAc)] 5H2O (11), whereas the 2:1 molar ratio reaction,..." @default.
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• W2053193516 date "1999-06-01" @default.
• W2053193516 modified "2023-10-16" @default.
• W2053193516 title "FEATURES OF A FLEXIBLE BACKBONE IN THE COORDINATION COMPOUNDS OF A DIOXIME LIGAND: THE CHARACTERIZATION OF SUPRAMOLECULAR AND DINUCLEAR METAL COMPLEXES" @default.
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• W2053193516 doi "https://doi.org/10.1080/00958979908024350" @default.
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