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- W2053204066 endingPage "90" @default.
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- W2053204066 abstract "A rapid and continuous hydrothermal route for the synthesis of nano-sized hydroxyapatite rods co-precipitated with calcium-doped zirconia nanoparticles using a superheated water flow at 450°C and 24.1 MPa as a crystallizing medium is described. Hydroxyapatite and calcium-doped zirconia phases in the powder mixtures could be clearly identified based on particle size and morphology under transmission electron microscopy. Retention of a nanostructure after sintering is crucial to load-bearing applications of hydroxyapatite-based ceramics. Therefore, rapid consolidation of the co-precipitates was investigated using a spark plasma sintering furnace under a range of processing conditions. Samples nominally containing 5 and 10 wt% calcium-doped zirconia and hydroxyapatite made with Ca:P solution molar ratio 2.5 showed excellent thermal stability (investigated using in situ variable temperature X-ray diffraction) and were sintered via spark plasma sintering to >96% sintered densities at 1000°C resulting in hydroxyapatite and calcium-doped zirconia as the only two phases. Mechanical tests of spark plasma sintering sintered samples (containing 10 wt% calcium-doped zirconia) revealed a three-pt flexural strength of 107.7 MPa and Weibull modulus of 9.9. The complementary nature of the spark plasma sintering technique and continuous hydrothermal flow synthesis (which results in retention of a nanostructure even after sintering at elevated temperatures) was hence showcased." @default.
- W2053204066 created "2016-06-24" @default.
- W2053204066 creator A5023720425 @default.
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- W2053204066 creator A5076786838 @default.
- W2053204066 creator A5079278198 @default.
- W2053204066 creator A5088633489 @default.
- W2053204066 date "2012-04-24" @default.
- W2053204066 modified "2023-09-23" @default.
- W2053204066 title "Phase stability and rapid consolidation of hydroxyapatite–zirconia nano-coprecipitates made using continuous hydrothermal flow synthesis" @default.
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