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- W2053224963 abstract "Abstract The tungsten hydrazido(2-) complex cis,mer-[WCl2(NNH2)(PMe2Ph)3], readily derived from a dinitrogen complex cis-[W(N2)2(PMe2Ph)4], reacted with 1,3,5-triketones RCOCH2COCH2COPh (R=Me, Ph) to give the diazoalkane complexes cis,mer-[WCl2(NNCRCH2COCH2COPh)(PMe2Ph)3] (R=Me (3), Ph) via the condensation between the hydrazido(2-) ligand and one terminal carbonyl group in the triketone. By contrast, the reaction of the hydrazido(2-) complex cis,trans-[WCl2(NNH2)(CO)(PMe2Ph)2] with PhCOCH2COCH2COPh resulted in the formation of a dinuclear μ-bis(diazoalkane) complex [WCl2(CO)(PMe2Ph)2(NNCPhCH2COCH2CPhNN)WCl2(CO)(PMe2Ph)2] (5). The structures of 3 and 5 in the solid state have been determined unequivocally by X-ray analysis." @default.
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- W2053224963 date "1999-02-01" @default.
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- W2053224963 title "Condensation of triketones with tungsten hydrazido(2-) complexes derived from a dinitrogen complex: formation of mononuclear or dinuclear diazoalkane complexes" @default.
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- W2053224963 doi "https://doi.org/10.1016/s0022-328x(98)00976-0" @default.
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