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- W2053280180 abstract "The production of high-purity ethyl acetate (EtAc) using reactive distillation (RD) is studied experimentally in a pilot-scale plant. The objectives are two folds: (1) to validate the appropriateness of the type-II RD flowsheet, a complex two-column configuration with liquid phase split, developed by Tang et al. (2005) and (2) to provide a startup procedure for continuous operation. This pilot-scale plant consists of one RD column and a downstream stripper with a decanter in between. The two columns are equipped with temperature, flow, and level measurements and control is executed in a Delta-V process control computer. The alcohol feed is of industrial grade ethyl alcohol (95.5 wt%; below azeotropic composition) and the acid feed contains 99wt% of acetic acid with water as impurity. Very stringent specification on EtAc is required: 99.00 wt% EtAc with acetic acid less than 100 ppm. Five experimental runs were performed and the results show that, with a correct start-up procedure, high-purity acetate can be produced in a straightforward manner." @default.
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- W2053280180 date "2007-01-01" @default.
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- W2053280180 title "Production of High-purity Ethyl Acetate using reactive distillation: Experimental Validation and Start-up procedure" @default.
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- W2053280180 doi "https://doi.org/10.3182/20070606-3-mx-2915.00062" @default.
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