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• W2053345150 abstract "Synthesis, crystal structure, thermal characterization, FTIR and Raman measurements are given for a new mixed compound cesium–ammonium tellurate. X-ray study showed that the [Cs0.92(NH4)0.08]2TeCl4Br2 compound crystallizes in the tetragonal space group P4/mnc, with a = 7.452 (1) A, c = 10.544 (3) A and Z = 2. The refinement converged at room temperature to Rp = 0.093 and Rwp = 0.076. The structure is considered as isolated octahedral TeCl4Br(_{2}^{2-}). These anions show a 4° rotation around the fourfold axis against the cubic arrangement of the K2PtCI6 type structure. The monovalent cations (Cs + /NH(_{4}^{+})) are located between the octahedra ensuring the stability of the structure by ionic and hydrogen bonding contacts: Cs...Cl/Br and N-H......Cl/Br. A DTA/TGA experiment at high temperature reveals one endothermic peak at 780 K for this compound. At low temperature a transition from phase I to phase II was detected at 213 K by DSC. This transition, confirmed by Raman analysis, can be attributed to an order–disorder phase transition." @default.
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• W2053345150 date "2012-03-01" @default.
• W2053345150 modified "2023-09-22" @default.
• W2053345150 title "Structural, thermal behaviour and vibrational study of a new mixed cesium–ammonium tellurate" @default.
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• W2053345150 doi "https://doi.org/10.1007/s12039-011-0146-8" @default.
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