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- W2053643509 abstract "4-O-Acetyl-1,6-anhydro-3-O-(4-methoxybenzoyl)-β-D -mannopyranose was converted in two steps into 4-O-acetyl-1,6-anhydro-2-deoxy-2-phthalimido-β-D-glucopyranose. Trimethylsilyl tri-fluoromethanesulphonate-catalysed coupling of 1,6-anhydro-2,3-O-(4-methoxybenzylidene)-β-D-mannopyranose with 1,3,4,6-tetra-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranose, followed by treatment with 2,3-dichloro-5,6-dicyano-1,4-benzoquinone, afforded the title compound. After triflation, the disaccharide thus obtained was treated with lithium azide or potassium phthalimide to afford 4-O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D- glucopyranosyl)-1,6-anhydro-2-azido-3-O-(4-methoxy-benzoyl)-2-deoxy -β-D-glucopyranose and 4-O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D -glucopyranosyl) −1,6-anhydro-2-deoxy-3-O-(4-methoxybenzoyl)-2-phthalimido-β- D-glucopyranose, respectively." @default.
- W2053643509 created "2016-06-24" @default.
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- W2053643509 date "1986-01-01" @default.
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- W2053643509 title "Synthesis of 4-O -(3,4,6-tri-O -acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-1,6-anhydro-3-O -(4-methoxybenzoyl)-β- D-mannopyranose: A versatile intermediate for the preparation of N,N -diacetylchitobiose derivatives" @default.
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- W2053643509 doi "https://doi.org/10.1002/recl.19861050407" @default.
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