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- W2053669563 abstract "The ionic complexes [Q][Ph2Sb(dmit)2] (4; Q = NEt4 or 1,4-Me2-pyridinium) and [Net4][(p-tolyl)2Sb(dmit)2] (5) have been prepared from [Q]2Zn(dmit)2] and Ar2SbCl3 in the presence of KSCN (H2-dmit = 4,5-dimercapto-1,3-dithiole-2-thione). As shown by X-ray crystallography for 4 (Q = NEt4) and 5, these complexes contain distorted octahedral anions with cis-aryl groups: The CSbC angles in 4 (Q = NEt4) and 5 are 93.1(2) adn 95.3(5)°, respectively. The dmit chealtes are unsymmetrically bonded to antimony in both 4 (Q = NEt4) and 5 with the longer bonds trans to the aryl groups (for both compounds, the SbS bond lengths are in the ranges, 2.614 to 2.636 and 2.530–2.550 Å)." @default.
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- W2053669563 date "1997-01-01" @default.
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- W2053669563 title "[Bis(1,3-dithiole-2-thione-4,5- dithiolato)diarylantimonate(1-)], [Ar2Sb(dmit)2]−, complexes. Crystal structures of [NEt4][Ar2Sb(dmit)2] (Ar = Ph or p-tolyl)" @default.
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- W2053669563 doi "https://doi.org/10.1016/s0277-5387(97)00004-1" @default.
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