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- W2053826187 abstract "Abstract A study on the microwave-assisted alcoholysis of diethyl phosphite with ethylene glycol revealed that after optimization of the conditions (molar ratio, temperature and time), the target “monomer,” (HOCH 2 CH 2 O) 2 P(O)H was formed in a proportion of 59 %, but with an incomplete conversion. The formation of the (HOCH 2 CH 2 O)(EtO)P(O)H and H(EtO)(O)POCH 2 CH 2 OP(O)(OEt)H by-products was, in most cases, inevitable. The alcoholysis with ethanolamine was more efficient and took place in a conversion of 100 % to afford H 2 NCH 2 CH 2 O) 2 P(O)H in a proportion of 85 %. An alkyl substituent on the N -atom prevented the alcoholysis." @default.
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- W2053826187 date "2014-11-01" @default.
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- W2053826187 title "Microwave-assisted alcoholysis of dialkyl phosphites by ethylene glycol and ethanolamine" @default.
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- W2053826187 doi "https://doi.org/10.1515/pac-2014-0601" @default.
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