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- W2053944480 abstract "Several isopolytungstates and similar compounds have been studied by proton magnetic resonance in D2O, in order to determine the number of non-exchangeable protons in their structure. The data confirm a basic form of metatungstate, i.e. HW12 O407−. The so-called “polytungstate X” is shown to be the β-isomer of metatungstate. Both forms of pseudometatungstate, namely Ψ′ and Ψ were studied and the formulae [HW12O39]5−·xH2O and [W12O396−·yH2O are proposed. The three following compounds [H2W12O39(O2)]6−·((O2) denoting the peroxidic group), [H2W12O39F]5− and [H2W12O38F2]4− derive from the metatungstic structure because each of them contains 2 non-exchangeable protons. Finally the effect of reduction upon the NMR spectrum of metatungstate is discussed." @default.
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- W2053944480 date "1976-01-01" @default.
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- W2053944480 title "High resolution PMR of several isopolytungstates and related compounds" @default.
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- W2053944480 doi "https://doi.org/10.1016/0022-1902(76)80402-2" @default.
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