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- W2054112814 abstract "Abstract Starting from 1,6-anhydro-β-D-mannopyranose, compounds 7a-d , which have a ketoxime ether at C3 and a carbon radical precursor tethered to the hydroxyl group at position 2, were efficiently prepared. While alkyl π-radicals derived from 7a and 7b failed to cyclize, the vinyl σ-radicals derived from 7c and 7d underwent the desired 1,5- exo cyclization, affording advanced precursors of (−)-tetrodotoxin. This type of transformation should be useful for the formation of sterically crowded nitrogen-bearing carbon centers in carbohydrate-derived substrates." @default.
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- W2054112814 date "1997-04-01" @default.
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- W2054112814 title "Radical cyclisation onto C-3 of 1,6-anhydro-β-d-mannopyranose derivatives. Application to the formation of the C8a centre of (−)-tetrodotoxin" @default.
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- W2054112814 doi "https://doi.org/10.1016/s0040-4039(97)00460-7" @default.
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