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- W2054175080 abstract "Starch-g-poly(methyl methacrylate) (PMMA) was prepared by emulsion photopolymerization without photoinitiator. Grafting efficiency was determined for two types of starch (high-amylose and amylopectin) and at several illumination times. Since clogging of the graft copolymer prevented vacuum filtration and Soxhlet extraction was too time-consuming, a new method to separate the PMMA homopolymer from the graft copolymer was developed. Back-flush filtration uses an intermittent pressure pulse to clean the filter as the homopolymer is separated from the graft copolymer. Back-flush filtration was shown to be more efficient by reducing the separation time and solvent use, and the grafting efficiencies obtained with back-flush filtration compare favorably with those from Soxhlet extraction for the starch-g-PMMA copolymer systems studied. More accurate grafting efficiencies could be obtained by applying a nonstick coating to the inside chamber of the back-flush filtration unit." @default.
- W2054175080 created "2016-06-24" @default.
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- W2054175080 date "2008-07-01" @default.
- W2054175080 modified "2023-09-26" @default.
- W2054175080 title "Evaluation of Novel Back‐flush Filtration for Removal of Homopolymer from Starch‐g‐PMMA" @default.
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- W2054175080 doi "https://doi.org/10.1002/star.200700709" @default.
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