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• W2054328238 abstract "The phase designated γ-Zn 3 (VO 4 ) 2 reported as a minor second phase in zinc oxide-based varistor materials doped with vanadium oxide and manganese oxide is shown to be the L phase, (Zn 1 − x Mn x ) 2 V 2 O 7 (0.188 < x < 0.538), in the pseudo-binary Mn 2 V 2 O 7 –Zn 2 V 2 O 7 system. Analysis of X-ray powder diffraction patterns and electron diffraction patterns of this phase shows that the previously published a , c and β values for this thortveitite-related phase are incorrect. Instead, Rietveld refinement of the X-ray powder pattern of the L phase shows that it has a monoclinic C lattice with Z = 6, with a = 10.3791 (1), b = 8.5557 (1), c = 9.3539 (1) Å and β = 98.467 (1)°. Although prior convergent-beam electron diffraction work of `γ-Zn 3 (VO 4 ) 2 ' confirmed the C Bravais lattice, the space group was found to be Cm rather than C 2/ m , the difference perhaps arising from the inability of the X-rays to detect small displacements of oxygen. Attempts to refine the structure in Cm did not produce improved R factors. The relationship between the crystal structure of the L phase and the high-temperature C 2/ m β′-Zn 2 V 2 O 7 thortveitite-type solid solution is discussed." @default.
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• W2054328238 date "2009-02-20" @default.
• W2054328238 modified "2023-10-16" @default.
• W2054328238 title "X-ray powder diffraction and electron diffraction studies of the thortveitite-related <i>L</i> phase, (Zn,Mn)₂V₂O₇" @default.
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• W2054328238 doi "https://doi.org/10.1107/s0108768108042444" @default.
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