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- W2054372268 abstract "Abstract The thiol-functionalised silsesquioxanes, [Si 8 O 12 (Pr n ) 7 (C 3 H 6 SH)], 1 , and [Si 8 O 12 (Pr n ) 6 { o- (C 3 H 6 SH) 2 }], 2 , (Pr n =C 3 H 7 ) readily react with the activated metal clusters [M 3 (CO) 10 (NCMe) 2 ] (M=Ru, Os) to form cluster-substituted silsesquioxanes. The compounds [Si 8 O 12 (Pr n ) 7 {( μ 2 -SC 3 H 6 )M 3 ( μ -H)(CO) 10 }] (M=Ru, 4 ; M=Os, 5 ) and [Si 8 O 12 (Pr n ) 6 { o- ( μ 2 -SC 3 H 6 )Ru 3 ( μ -H)(CO) 10 } 2 ] 6 have been prepared and characterized. The octa-substituted silsesquioxane, [Si 8 O 12 (C 3 H 6 SH) 8 ], 3 , may be partially or completely substituted at its thiol functionalities depending on the reaction stoichiometry employed; [Si 8 O 12 (C 3 H 6 SH) 6 {( μ 2 -SC 3 H 6 )Ru 3 ( μ -H)(CO) 10 } 2 ], 7 , and [Si 8 O 12 {( μ 2 -SC 3 H 6 )Ru 3 ( μ -H)(CO) 10 } 8 ], 8 , have been prepared." @default.
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- W2054372268 title "Reactions of thiol-functionalized silsesquioxanes with metal carbonyl clusters: syntheses and characterization of [Si8O12(Prn)7{(μ2-SC3H6)M3(μ-H)(CO)10}] (M=Ru, Os; Prn=C3H7), [Si8O12(Prn)6{(μ2-SC3H6)Ru3(μ-H)(CO)10}2] and [Si8O12(C3H6SH)x{(μ2-SC3H6)Ru3(μ-H)(CO)10}8−x] (x=6, 0)" @default.
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