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- W2054432810 abstract "N-Trifluoroacetyl-l-norvalyl-l-norvaline1 cyclohexyl ester has been synthesized in high yield and used as a stationary phase for the gas chromatographic enantiomeric separation of N-trifluoroacetyl-d,l-amino acid isopropyl esters. Separation factors and enthalpies of solution have shown a marked increase on solute-solvent interaction to occur for α-amino acids with a four-carbon group on the asymmetric carbon, while the same factors decrease as the substituent grows from one- to three-carbon. Mixtures of d,l-serine and d,l-leucine can now be resolved. Earlier phases have shown significant overlap between d isomers of leucine and serine as well as their l isomers, thereby precluding an accurate qualitative analysis of naturally occurring volatile amino acid derivatives. The phase has also been examined with respect to the separation of a mixture of common amino acids and their enantiomers and was found to be satisfactory." @default.
- W2054432810 created "2016-06-24" @default.
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- W2054432810 date "1972-05-01" @default.
- W2054432810 modified "2023-10-16" @default.
- W2054432810 title "N-trifluoroacetyl-l-norvalyl-l-norvaline cyclohexyl ester as a stationary phase and its interaction with asymmetric solutes" @default.
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- W2054432810 doi "https://doi.org/10.1016/s0021-9673(01)91225-7" @default.
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