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• W2055005166 abstract "Abstract Copolymerizations of a six‐membered ring spiro‐orthocarbonate bearing adamantane backbones ( AD ‐ SOC , 1 ) and a monofunctional epoxide, PGE , in the presence of cationic initiators such as Sc(OTf) 3 were carried out under various reaction conditions. As a result, instead of the anticipated poly(ether‐ether‐carbonate) 11 , two types of copolyethers ( 12 and 18 ) consisting of two or three types of ether components having different substituent groups were unusually formed along with the evolution of carbon dioxide gas, in which AD ‐ SOC efficiently acted as the corresponding oxetane equivalent monomers 3 and 4 . Furthermore, the copolymerization behavior, including the formation of copolyethers 12 and 18 , unexpectedly and significantly depended on the reaction conditions, such as the concentration of the initiator. For example, the copolymerizations with 5 mol % of Sc(OTf) 3 mainly afforded copolyether 18 , while those with 1 mol % mainly gave copolyether 12 . In addition, treatments with 5 mol % of Sc(OTf) 3 also yielded CH 2 Cl 2 , THF, and DMF‐insoluble networked products, indicating relatively higher thermal stability compared with a common polyether. © 2005 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem 43: 1729–1740, 2005" @default.
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• W2055005166 date "2005-03-08" @default.
• W2055005166 modified "2023-10-18" @default.
• W2055005166 title "Unusual cationic copolymerization behavior of a six-membered ring spiro-orthocarbonate bearing adamantane backbones with a monofunctional epoxide" @default.
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• W2055005166 doi "https://doi.org/10.1002/pola.20633" @default.
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