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• W2055098669 abstract "The synthesis and characterization of chromium basic carboxylate complexes, [Cr3(O2CR)6L3]+, containing trifluoroacetate, 3-fluoropyridine, 3-trifluoromethylpyridine, and 4-trifluoromethylpyridine are described. The substituted pyridine ligands are used as models of DNA bases to determine whether 19F NMR would be a potentially useful probe of the binding of Cr3+ to DNA. The 19F NMR resonances of the coordinated ligands, while broadened by delocalization of unpaired electron density from the S=3/2 chromic centers, are readily discernable, and the contact shifts are of sufficient magnitude that the signals from coordinated and free ligands can easily be differentiated. Thus, 19F NMR appears to be a potentially useful probe of the binding of Cr3+ to DNA containing F-labeled bases. Additionally, electrospray MS is shown to be a convenient method to establish the identity of chromium basic carboxylate assemblies." @default.
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• W2055098669 date "2013-11-01" @default.
• W2055098669 modified "2023-10-11" @default.
• W2055098669 title "Paramagnetic 19F NMR and electrospray ionization mass spectrometric studies of substituted pyridine complexes of chromium(III): Models for potential use of 19F NMR to probe Cr(III)–nucleotide interaction" @default.
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• W2055098669 doi "https://doi.org/10.1016/j.poly.2013.03.002" @default.
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