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• W2055143596 abstract "In this study the rapid growth of sII H2 hydrate within 20 min of post formation quenching towards liquid nitrogen (LN2) temperature is presented. Initially at 72 MPa and 258 K, hydrate samples would cool to the conditions of ∼60 MPa and ∼90 K after quenching. Although within the stability region for H2 hydrate, new hydrate growth only occurred under LN2 quenching of the samples when preformed hydrate “seeds” of THF + H2 were in the presence of unconverted ice. The characterization of hydrate seeds and the post-quenched samples was performed with confocal Raman spectroscopy. These results suggest that quenching to LN2 temperature, a common preservation technique for ex situ hydrate analysis, can lead to rapid unintended hydrate growth. Specifically, guest such as H2 that may otherwise need sufficiently long induction periods to nucleate, may still experience rapid growth through an increased kinetic effect from a preformed hydrate template." @default.
• W2055143596 created "2016-06-24" @default.
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• W2055143596 date "2012-06-20" @default.
• W2055143596 modified "2023-09-26" @default.
• W2055143596 title "Rapid hydrogen hydrate growth from non-stoichiometric tuning mixtures during liquid nitrogen quenching" @default.
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• W2055143596 doi "https://doi.org/10.1063/1.4729473" @default.
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