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- W2055164598 abstract "An analytical method for the determination of norethisterone acetate (NETA) in human plasma by capillary gas chromatography-mass-selective detection (GC-MS), with testosterone acetate as internal standard, was developed and validated. After addition of the internal standard, the compounds were extracted from plasma at basic pH into diethyl ether-dichloromethane (3:2 v/v), which was then evaporated to dryness. The compounds were converted into their pentafluoropropionyl derivatives which were determined by gas chromatography using a mass selective detector at m/z 486 for NETA and m/z 476 for the internal standard. Intra-day and inter-day accuracy and precision were found suitable over the range of concentrations between 0.10 to 10 ng/ml. The method was applied to clinical samples." @default.
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- W2055164598 date "1996-10-01" @default.
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- W2055164598 title "Quantitative determination of norethisterone acetate in human plasma by capillary gas chromatography with mass-selective detection" @default.
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- W2055164598 doi "https://doi.org/10.1016/0021-9673(96)00483-9" @default.
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