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• W2055173824 abstract "A novel three-dimensional (3D) mixed-valence iron coordination polymer [Fe2IIIFeIIO2(IN)2(ox)] (IN=isonicotinate, ox=oxalate) (1) has been hydrothermally synthesized by using two different anionic ligands and characterized by elemental analysis, IR spectrum, electron spin resonance (ESR), X-ray photoelectron spectrum (XPS), thermogravimetric analysis (TGA) and single crystal X-ray diffraction. Compound 1 crystallizes in the monoclinic, space group P2(1)/c with a=5.8774(7) Å, b=18.528(2) Å, c=7.7117(9) Å, β=103.168(2)Å, V=817.69(17) Å3, Z=2, and R1=0.0321 (wR2=0.0777). The Fe(II) and Fe(III) centers in 1 both exhibit a distorted octahedral coordination geometry and are bridged by the IN and oxalate groups into a covalently bonded 3D metal–organic network. TGA showed that the 3D network possesses a good stability up to 291 °C." @default.
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• W2055173824 date "2003-05-01" @default.
• W2055173824 modified "2023-10-17" @default.
• W2055173824 title "Hydrothermal synthesis and crystal structure of a novel three-dimensional mixed-valence iron coordination polymer [Fe2IIIFeIIO2(IN)2(ox)] (IN=isonicotinate, ox=oxalate)" @default.
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• W2055173824 doi "https://doi.org/10.1016/s0022-2860(03)00149-2" @default.
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