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- W2055175518 startingPage "1077" @default.
- W2055175518 abstract "A cobalt(III) complex with the sexidentate ligand, N,N′-ethylenebis(S-methyl-L-cysteine), was newly synthesized and chromatographically isolated. Of two possible geometrical isomers, trans(O) and trans(N), one isomer was formed selectively. The dark-red crystals are orthorhombic, space group P212121, a=9.055(2), b=22.123(7), c=17.111(4) A, and Z=8. The structure was solved by the direct method and refined to R=0.066 for 2380 nonzero reflections. The complex is trans(O) isomer and the crystal consists of two kinds of complex cations with respect to the absolute configurations of the coordinated asymmetric sulfur atom. One takes an S(S),S(S) configuration and the other an R(S),S(S) one. The changes in configuration between the asymmetric sulfur atoms in the crystal and those in aqueous solution are discussed on the basis of NMR (13C and 1H) spectral studies." @default.
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- W2055175518 date "1982-04-01" @default.
- W2055175518 modified "2023-09-25" @default.
- W2055175518 title "Characterization of<i>trans</i>(<i>O</i>)-<i>N</i>,<i>N</i>′-Ethylenebis(<i>S</i>-methyl-L-cysteinato)cobalt(III) Perchlorate and the Absolute Configuration of the Complex Determined by X-Ray Analysis" @default.
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- W2055175518 doi "https://doi.org/10.1246/bcsj.55.1077" @default.
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