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- W2055186115 abstract "Two dynamic chiral stationary phases CSP 7 and 12) were prepared starting from R-2-amino-1-propanol and (R)-α-phenylethylamine. The resolution of racemic α-amino acids on the two dynamic CSPs thus prepared were compared with previously reported resolution data on a dynamic CSP (2) derived from (1S,2R)-norephedrine. The enantioselectivity for the two enantiomers of α-amino acids on CSP 7 was found to be comparable to or better than that on CSP 2 while the enantioselectivity for the two enantiomers of α-amino acids on CSP 12 was much worse than that on CSPs 2 or 7. From these results, we concluded that the phenyl functionality at the first chiral center of CSP 2 is not essential in the chiral recognition. However, the hydroxy functionality of CSPs 2 or 7 does play a very important role in the chiral recognition." @default.
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- W2055186115 date "1994-11-01" @default.
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- W2055186115 title "Mechanistic evaluation of the resolution of α-amino acids on dynamic chiral stationary phases derived from amino alcohols by ligand-exchange chromatography" @default.
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- W2055186115 doi "https://doi.org/10.1016/0021-9673(94)00595-8" @default.
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