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- W2055277568 abstract "Abstract Previously an acceptable precision (coefficient of variation less than 10%) could be obtained only part of the time for the peak areas of derivatized iodothyronine standards, even relative to that of a structurally close internal standard, 3,4-diiodo-3′,5′-dibromothyronine, when these compounds were analyzed at the low picogram level by capillary gas chromatography with electron-capture detection. This problem has now been ovecome, primarily by introducing a new design, material and conditioning of a direct vapor-injector insert. An extensive analysis under practical operating conditions of derivatized 3,5-di-, 3,5,3′-tri and 3,5,3′,5′-tetraiodothyronine at the 5-10-pg level, involving several changes in the injection equipment and several days of injections, now gives within-day coefficients of variation ranging from 2.7 to 7.7%, 1.5 to 5.3% and 1.8 to 5.2%, respectively, for the relative peak areas of these compounds." @default.
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- W2055277568 date "1982-05-01" @default.
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- W2055277568 title "Precision at the low picogram level in the analysis of derivatized iodothyronine standards by capillary gas chromatography with electron-capture detection" @default.
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- W2055277568 doi "https://doi.org/10.1016/s0021-9673(00)99621-3" @default.
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