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- W2055337439 abstract "Reactive sintering of 3 Ti : Sn :2 C and 3Ti:Sn:2C:0.6Fe powder mixtures is studied in the temperature range 510°C–1200°C under argon. It is demonstrated that the recently discovered Ti 3 SnC 2 phase is formed, provided that Fe is added to a 3 Ti : Sn :2 C reactant mixture within the synthesis conditions used. Using dilatometric and X ‐Ray diffraction analyses, the formation mechanism of Ti 3 SnC 2 is discussed. Results show that at low temperature (about 510°C), tin is consumed to form Fe x Sn y intermetallics. At high temperature (about 1060°C), tin is newly available to form Ti 3 SnC 2 due to the melting of Fe x Sn y . Then, the intermediate phases, TiC and Ti 2 SnC , and/or Ti 5 Sn 3 , TiC , C , and Ti are dissolved in the ( Fe + Sn ) liquid phase and Ti 3 SnC 2 very likely precipitate from the melt. The second part of the study deals with the optimization of the Fe content in the initial 3Ti:Sn:2C reactant powder mixture to synthesize samples with larger Ti 3 SnC 2 content by hot isostatic pressing." @default.
- W2055337439 created "2016-06-24" @default.
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- W2055337439 date "2013-06-05" @default.
- W2055337439 modified "2023-10-03" @default.
- W2055337439 title "Formation Mechanisms of Ti<sub>3</sub> SnC<sub>2</sub> Nanolaminate Carbide Using Fe as Additive" @default.
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- W2055337439 doi "https://doi.org/10.1111/jace.12427" @default.
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