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- W2055356492 abstract "The interactions between 2,6-diacetylpyridine bis-4- N -ethylthiosemicarbazone ( 1 ) and ten lanthanide triflates have been studied by means of electrospray ionization mass spectrometry. The aim of this work is to gain a better insight into the coordination trends of thiosemicarbazones towards lanthanides. Thiosemicarbazone ligand 1 forms with lanthanides stable complexes, which can be observed in the ESI spectra. The lanthanide salts, trifluoromethanesulfonates(triflates) La(CF 3 SO 3 ) 3 , and the ligand, 2,6-diacetylpyridine bis-4- N -ethylthiosemicarbazone 1 , in acetonitrile were infused into the ESI source and positive mass spectra have been obtained. ► Electrospray ionization mass spectra of solutions containing thiosemicarbazone, lanthanide triflate and acetonitrile. ► Thiosemicarbazone-lanthanide complexes detected and their structure analyzed. ► Ligand's affinity to fluoride anions confirmed. ► Thiosemicarbazone/lanthanide triflates complexation mainly through deprotonation of the ligand." @default.
- W2055356492 created "2016-06-24" @default.
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- W2055356492 date "2012-06-01" @default.
- W2055356492 modified "2023-09-24" @default.
- W2055356492 title "Electrospray ionization mass spectrometry of lanthanide(III) complexes with 2,6-diacetylpyridine bis-4-N-ethylthiosemicarbazone" @default.
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- W2055356492 doi "https://doi.org/10.1016/j.inoche.2012.02.016" @default.
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