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- W2055366949 abstract "Reaction of MCl2 (M Mn, Fe, Co, Ni, Cu, Zn) and MCl3 (M Ti, V, Cr, Fe) with diethyl 6-methylpyridine-2-phosphonate at elevated temperatures results in the precipitation of ethoxy 6-methylpyridine-2-phosphonate (E6MPP) metal complexes. Spectral evidence suggests that, in these compounds, E6MPP acts as a bidentate N,0-chelating agent. The new complexes were characterized by means of spectral and magnetic studies; the following structures are proposed: [M(E6MPP)2]2 (M Mn, Fe, Co, Ni): pentacoordinated, binuclear chelates containing two bridging and two terminal E6MPP ligands; one -POO oxygen acts as the bridging group in these complexes (M O M bridges); M(E6MPP)2 (M Cu, Zn): monomeric chelates, involving tetrahedral MO2N2 moieties; M(E6MPP)3 monomeric, distorted octahedral chelates, and Fe(E6MPP)2Cl, involving either a monomeric, pentacoordinated or a binuclear, chlorine bridged, hexacoordinated structure. The mechanism of formation of the new complexes is discussed, and preliminary data on the products of the reaction between 3d metal dichlorides and diethyl pyridine- and 4-methylpyridine-2-phosphonates are presented." @default.
- W2055366949 created "2016-06-24" @default.
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- W2055366949 date "1973-06-01" @default.
- W2055366949 modified "2023-09-27" @default.
- W2055366949 title "Ethoxy 6-methylpyridine-2-phosphonato complexes with 3d metal ions" @default.
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- W2055366949 doi "https://doi.org/10.1016/0022-1902(73)80118-6" @default.
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