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• W2055400169 abstract "The cyanoacetylide complex Fe(C≡CC≡N)(dppe)Cp (3) is readily obtained from sequential reaction of Fe(C≡CSiMe 3 )(dppe)Cp with methyllithium and phenyl cyanate. Complex 3 is a good metalloligand, and coordination to the metal fragments [RhCl(CO) 2 ], [Ru(PPh 3 ) 2 Cp] + , and [Ru(dppe)Cp*] + affords the corresponding cyanoaceylide-bridged heterobimetallic complexes. In the case of the 36-electron complexes [Cp(dppe)Fe-C≡CC≡N-ML n ] n + , spectroscopic and structural data are consistent with a degree of charge transfer from the iron centre to the rhodium or ruthenium centre via the C 3 N bridge, giving rise to a polarized ground state. Electrochemical and spectroelectrochemical methods reveal significant interactions between the metal centres in the oxidized (35 electron) derivatives, [Cp(dppe)Fe-C≡CC≡N-ML n ] (n+1)+ . Key words: cyanide, cyanoacetylide, crystal structure." @default.
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• W2055400169 date "2006-02-01" @default.
• W2055400169 modified "2023-10-18" @default.
• W2055400169 title "The synthesis, structure, and electrochemical properties of Fe(C≡CC≡N)(dppe)Cp and related compounds" @default.
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• W2055400169 doi "https://doi.org/10.1139/v05-238" @default.
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