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• W2055476454 startingPage "101" @default.
• W2055476454 abstract "A new [3 + 3] Schiff base macrocycle incorporating three N2O2 salphen-type binding sites and peripheral neopentyloxy substituents has been prepared. The incorporation of Zn2+ ions into this and related conjugated Schiff base macrocycles has been studied by NMR spectroscopy, mass spectrometry, and X-ray diffraction. When reacted with 7 equiv of zinc acetate, the macrocycles template the formation of heptanuclear complexes. Two tetranuclear Zn2+ complexes that are plausible intermediates in the assembly of the heptanuclear complexes have been isolated and structurally characterized. These reactive intermediates are promising substrates for the synthesis of polynuclear, mixed-metal clusters. We also demonstrate that this chemistry may be generalized to other bridging carboxylate ligands, such as methacrylate." @default.
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• W2055476454 date "2007-12-08" @default.
• W2055476454 modified "2023-10-16" @default.
• W2055476454 title "Zinc Carboxylate Cluster Formation in Conjugated Metallomacrocycles: Evidence for Templation" @default.
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• W2055476454 doi "https://doi.org/10.1021/ic701385m" @default.
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