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- W2055652783 abstract "Abstract The title compounds are prepared from trichloromethylphosphonic acid dichloride and excess hydrazine hydrate, and from the dihydrazide and the dichloride in the presence of triethylamine, resp. They are characterized by elemental analysis, mass spectra, 1 H and 31 P NMR spectra, IR and Raman data. Thin layer chromatographic experiments show that in the raw material of the ring compound two isomers (probably cis- and trans-) are present, whereas in the recrystallized product only one isomer can be detected. Attempts of a preparative separation of isomers were unsuccessfull so far due to very low concentrations of the product with the slightly higher R f . Single crystals of the isolated ring compound decompose on irradiation with X-rays" @default.
- W2055652783 created "2016-06-24" @default.
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- W2055652783 date "1982-02-01" @default.
- W2055652783 modified "2023-09-26" @default.
- W2055652783 title "Trichonnethylphosphonsäuredihydrazid und 3.6-Bi8(trichlormethyl)-3.6-dioxo-1.2.4.5-tetraaza-3.6-diphosphacyclohexan / Trichloromethylphosphonic Acid Dihydrazide and 3,6-Bis(trichloromethyl)-3,6-dioxo-1,2,4,5-tetraaza-3,6-diphosphacyclohexane" @default.
- W2055652783 doi "https://doi.org/10.1515/znb-1982-0213" @default.
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