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- W2055837919 abstract "Fine, whisker-like crystals of Rb2Fe5F17 have been obtained from solid state stoichiometric mixtures of RbF and FeF3. A structural model has been determined from single crystal diffractometer data in the Fmmm orthorhombic space group : a = 14.887(2) Å, b = 25.814(3) Å, c = 7.560(1) Å; z = 8; ϱexp. = 3.529 g cm−3; ϱcalc.=3.535 g cm−3; λCo Ka=1.7903 Å; R = 0.068; Rω = 0.096 for 175 reflections with Iσ(I) > 6. The structure has been compared with that of HTB. Rb2Fe5F17 exhibits layers of (Fe5F17)2n−n composition containing FeF6 corned-shared octahedra forming tunnels of hexagonal and triangular sections. Rubidium atoms are located between the layers and within the hexagonal tunnels with statistical occupancy. The structure has been roughly confirmed by TEM. The observed lowering in symmetry from Fmmm may be explained by partial ordering of rubidium and by possible bridging of (Fe5F17) sheets by FeF6 octahedra." @default.
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- W2055837919 date "1990-03-01" @default.
- W2055837919 modified "2023-09-25" @default.
- W2055837919 title "Crystal structure of Rb2Fe5F17" @default.
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- W2055837919 doi "https://doi.org/10.1016/0025-5408(90)90103-9" @default.
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