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• W2055897338 abstract "Cyclo-1,3-dien-5-ynes with ring sizes from 10 to 14 (6 a–e) have been prepared for the first time by using a five-step synthesis starting from the alkynols 7 a–e. The final ring-closure was achieved by McMurry coupling of the α,ω-dialdehydes 12 a–e with the complex TiCl3(DME)1.5. Thermal isomerization of the cyclodienynes leads to the corresponding benzocycloalkenes, and it has been shown that the ring size has a considerable influence on the temperature necessary for thermocylization." @default.
• W2055897338 created "2016-06-24" @default.
• W2055897338 creator A5048836127 @default.
• W2055897338 creator A5061216831 @default.
• W2055897338 date "2001-10-15" @default.
• W2055897338 modified "2023-09-23" @default.
• W2055897338 title "Synthesis of Cyclo-1,3-dien-5-ynes" @default.
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• W2055897338 doi "https://doi.org/10.1002/1521-3765(20011015)7:20<4378::aid-chem4378>3.0.co;2-i" @default.
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