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• W2055966029 abstract "Silver bis(3,5,5-trimethyl-l-hexyl) sulfosuccinate, Ag-AOT-TMH, exhibits 1.2 wt % solubility in dense CO 2 at 40 °C and 52 MPa. This is a remarkably high CO 2 solubility value for a nonfluorous organometallic compound. Silver nanoparticles were produced by reducing the supercritical CO 2 solution containing 0.06 wt % Ag-AOT-TMH and 0.5 wt % perfluorooctanethiol (stabilizing ligand) using a reducing agent of NaBH 4 . Silver nanoparticles ranging in size from 1 to 6 nm were characterized by transmission electron microscopy (TEM) and energy-dispersive spectroscopy (EDS). Although silver nanoparticles have been previously formed by a similar technique using silver acetylacetonate, that precursor is far less CO 2 -philic, exhibiting a CO 2 solubility of «0.01 wt % at 40 °C and 70 MPa. Attempts to produce silver nanoparticles from Ag-AOT-TMH in a completely nonfluorous system were unsuccessful because stabilization could not be attained with silicone-, PEG-, or hydrocarbon-based thiols; only the fluorinated thiols provided nanoparticle dispersion." @default.
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• W2055966029 date "2006-01-21" @default.
• W2055966029 modified "2023-09-25" @default.
• W2055966029 title "Preparation of Silver Nanoparticles via Reduction of a Highly CO₂-Soluble Hydrocarbon-Based Metal Precursor" @default.
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• W2055966029 doi "https://doi.org/10.1021/ie050684p" @default.
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