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- W2056088770 abstract "Abstract Summary: N ‐Propargylamide‐terminated peptide‐based macromonomers with a degree of polymerization ranging from 4 to 40 were synthesized by the polymerization of γ ‐benzyl and γ ‐stearyl‐ L ‐glutamate‐ N ‐carboxy anhydrides initiated with propargylamine. The macromonomers took an α ‐helical structure, which was confirmed by signals at 208 and 220 nm in CD spectra. The macromonomers were subjected to polymerization and copolymerization with an alanine‐derived N ‐propargylamide [ N ‐( tert ‐butoxycarbonyl)‐ L ‐alanine‐ N′ ‐propargylamide] catalyzed with (2,5‐norbornadiene)Rh + [ η 6 ‐C 6 H 5 B − (C 6 H 5 ) 3 ]. It was confirmed through a CD spectroscopic study that the copolymer obtained from the copolymerization of the γ ‐stearyl‐ L ‐glutamate‐based macromonomer with the alanine‐derived N ‐propargylamide had a helical polyacetylene main chain and helical polypeptide side chains. magnified image" @default.
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- W2056088770 date "2004-06-17" @default.
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- W2056088770 title "Helical Polymer Carrying Helical Grafts from Peptide-Based Acetylene Macromonomers: Synthesis" @default.
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- W2056088770 doi "https://doi.org/10.1002/mabi.200400019" @default.
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