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- W2056173823 abstract "Man erhält die Substanzen in kristallinerform durch Umsetzung der reinen Alkalimetalle mit den Chalkogenen in flüssigem Ammoniak im Molverhältnis 2:3 bei Drucken bis zu 3000 bar und Temperaturen um 600 K. Sie kristallisieren alle im K2S3-Typ (Raumgruppe Cmc21 (Nr. 36)). Ihre Gitterkonstanten lauten: Das charakteristische Merkmal der Struktur sind die gewinkelten Chalkogenid-Polyanionen X32−. Die neu beschriebenen Verbindungen werden mit den anderen bis jetzt bekannten Dialkalimetall-trichalkogeniden verglichen. Preparation and Crystal Structure of the Dialkali Metal Trichalcogenides Rb2S3, Rb2Se3, Cs2S3, and Cs2Se3 Crystalline products were obtained by the reaction of the pure alkali metals with the chalcogens in the molar ratio 2:3 in liquid ammonia at pressures up to 3000 bar and temperatures around 600 K. The substances crystallize in the K2S3 type structure (space group Cmc21(NO. 36)). Unit cell constants see „Inhaltsübersicht”︁. The characteristic feature of this structure are bent polyanions X32−:(X = S,Se). The new described compounds are compared with the other known alkali metal trichalcogenides." @default.
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- W2056173823 date "1980-02-01" @default.
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- W2056173823 title "Darstellung und Kristallstruktur der Dialkalimetalltrichalkogenide Rb2S3, Rb2Se3, Cs2S3 und Cs2Se3" @default.
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- W2056173823 doi "https://doi.org/10.1002/zaac.19804610103" @default.
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