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- W2056260193 abstract "The 6α,7α-diol grouping in methyl hyocholate readily yields cyclic alkanebo-ronate esters, which are stable enough to permit some separate reactions of the 3α-hydroxy group, but which can be solvolysed to regenerate the diol. Mono-derivatives such as methyl hyocholate 3-acetate, so obtained, are of potential value in the preparation of a variety of “mixed” derivatives, and also of 6,7-seco-steroids of the 5β-H series. Gas chromatographic and mass spectrometric data are reported for eleven derivatives of methyl hyocholate, and the corresponding 6,7-seco-dialdehyde is characterized in the form of dioxime derivatives. Retention indices (OV-1) are reported for five derivatives of each of three isomers of methyl hyocholate: the 5β-3α,6β,7β-triol, 5α-3α,6α,7α-triol and 5α-3α,6β,7β-triol. Some distinctive features of the electron impact (70 eV) mass spectra are illustrated for the 3-trimethylsilyl ether 6,7-methaneboronates of these isomers." @default.
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- W2056260193 date "1984-04-01" @default.
- W2056260193 modified "2023-09-24" @default.
- W2056260193 title "Studies of the selective derivatization of methyl hyocholate and related steroidal ring b diols by gas chromatography-mass spectrometry" @default.
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- W2056260193 doi "https://doi.org/10.1016/s0021-9673(00)95091-x" @default.
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