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• W2056510888 abstract "The syntheses, structures, and magnetic properties of four heterometallic dodecanuclear aggregates with molecular formulas [NiΙΙ8REΙΙΙ4(L)8(CO3)6(H2O)14]·mCH3OH·12H2O [RE = Gd (1), m = 2; Dy (2), m = 0] and [NiΙΙ8REΙΙΙ4(L)8(CO3)4(CH3OH)4(H2O)8]·(ClO4)4·8H2O [RE = Dy (3), Y (4)] are presented. These complexes were obtained from two easy synthetic procedures through atmospheric CO2 fixation involving direct reaction of 2-(2-hydroxy-3-methoxybenzylideneamino)phenol (H2L) with RE(NO3)3·nH2O and Ni(ClO4)2·6H2O in the presence of triethylamine in different solvents under ambient conditions. Single-crystal X-ray diffraction reveals that these complexes possess very similar core structures featuring an unprecedented “tetra-capped hexahedron” topology bridged by four μ5-bridged carbonates. Static magnetic susceptibility measurements indicate dominant ferromagnetic coupling between the metal centers for 1 and 4. The dissimilar static and dynamic magnetic behaviors seen in 2 and 3 are probably ascribed to different coordination environments and ligand fields around DyΙΙΙ ions. These complexes represent limited examples of high-nuclearity NiΙΙ-REΙΙΙ family trapping μ5-bridged carbonates through atmospheric carbon dioxide fixation." @default.
• W2056510888 created "2016-06-24" @default.
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• W2056510888 date "2015-01-23" @default.
• W2056510888 modified "2023-10-07" @default.
• W2056510888 title "Synthesis, structures, and magnetic properties of four dodecanuclear Ni₈RE₄ (RE = Gd, Dy, Y) clusters trapping four μ₅-bridged carbonate anions" @default.
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• W2056510888 doi "https://doi.org/10.1080/00958972.2015.1004326" @default.
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