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- W2056513014 abstract "Mononuclear cyclopalladated complexes of type PdCl(Ph2N-N=CR1-C-R2=N-NPh2), where R1=R2=H (2a), R1=R2=CH3 (2b), and R1=H, R2=CH3 (2c) were synthesized by the reaction of palladium chloride and hydrazones. Additionally, the reaction of the complex 2c towards lithium phenylacetylide was studied, giving Ph2N—N=C(CH3)—CH=N—N(Ph)(o-C6H4—C≡C—Ph) (3). The complexes 2a-2c and compound 3 were characterized by IR, Mass, 1H, 13C, and 2D NMR spectroscopy. X-ray structure of complex 2c was also determined. Cyclopalladierte Komplexe durch Transmetallierungsreaktion mit Diphenylhydrazonen Einkernige Palladiumkomplexe der Art PdCl(Ph2N-N=CR1-C-R2=N-NPh2), mit R1=R2=H (2a), R1=R2=CH3 (2b) und R1=H, R2=CH3 (2c) wurden durch Reaktion von Palladiumchlorid mit Hydrazonen dargestellt. Zusätzlich wurde die Reaktion des Komplexes 2c mit Lithiumphenyl acetylid untersucht, die Ph2N—N=C(CH3)—CH=N—N(Ph)(o-C6H4—C≡C—Ph) (3) ergab. Die Komplexe 2a-c und die Verbindung 3 wurden durch IR-, Massen-, 1H-, 13C- und 2D-Spektroskopie charakterisiert. Eine Röntgenstrukturanalyse von 2c wurde ebenfalls vorgenommen." @default.
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- W2056513014 date "2002-09-01" @default.
- W2056513014 modified "2023-10-17" @default.
- W2056513014 title "Cyclopalladated Complexes Derived from Diphenylhydrazones and their Transmetallation Reaction" @default.
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- W2056513014 doi "https://doi.org/10.1002/1521-3749(200209)628:9/10<2104::aid-zaac2104>3.0.co;2-a" @default.
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