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- W2056517024 abstract "Abstract We have synthesized structurally reinforced chiral pentaaza-fifteen-membered polyamines 1 and 2 with a dibridge for the purposes of studying the size-match selectivity of the macrocyclic cavity. Particularly, an attempt has been made to synthesize copper(II) complexes of 1 and 2 to characterize the size-match selectivity of the polyamines in term of microscopic details of the metal-ion binding site. For this purpose the use of ESR spectroscopy has been invoked before X-ray structural analyses of the complexes are carried out. Powder-pattern ESR spectra of the copper(II) complex of 1 in crystalline solid have revealed a temperature dependence of the copper hyperfine structure. This finding suggests that a vibronic effect features in the hyperfine spectra, showing that the pentaaza-macrocycle under study accommodates copper(II) ion and the macrocycle is flexible to exert “genuine” size-match selectivity." @default.
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- W2056517024 date "1996-03-01" @default.
- W2056517024 modified "2023-09-23" @default.
- W2056517024 title "Structurally Reinforced Chiral Macrocyclic Polyamine Copper (II) Complexes as Studied by ESR and Squid Measurements" @default.
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- W2056517024 doi "https://doi.org/10.1080/10587259608033680" @default.
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