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- W2056531467 abstract "p-[Tris(p-t-butylphenyl)methyl]phenoxymethylstyrene (10) was prepared as a mixture of meta and para isomers via Williamson ether synthesis from vinylbenzyl chloride. Monomer 10 polymerizes smoothly under free-radical conditions. Under anionic polymerization conditions, nucleophilic attack at the benzylic position displaces the substituted phenoxide ion; by using an excess of n-butyllithium, however, a polymer of complex structure, high molecular weight and polydispersity of 2.2 was formed. On the basis of its steric bulk and polymerizability, new monomer 10 is therefore a useful in-chain ‘knot’ or ‘stopper’ for polyrotaxane synthesis using free-radical techniques, but not via anionic methods." @default.
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- W2056531467 date "1995-01-01" @default.
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- W2056531467 title "Synthesis and polymerization of a bulky styrenic monomer as an in-chain ‘knot’ for polyrotaxanes" @default.
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- W2056531467 doi "https://doi.org/10.1016/0032-3861(95)91209-p" @default.
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