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• W2056561441 abstract "We present a new analytical procedure for the extraction and determination of natural estrogens in soils based on pressurised liquid extraction and GC-MS determination. After testing twelve solvents, acetone proved to be the most efficient extractant. The optimum extraction temperature is 60 degrees C. Soil extracts have to be purified and concentrated by C-18 solid phase extraction. The dried extracts are derivatised by N-methyl-N-(trimethylsilyl)trifluoro-acetamide before measurement by GC-MS. Recoveries of 79-103% with relative standard deviations <or=13% document reliability of this method. Further, rapidity of extraction and a low detection limit (1 ng kg(-1)) represent an improvement of estrogen analysis in soils compared to established procedures." @default.
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• W2056561441 date "2008-03-01" @default.
• W2056561441 modified "2023-10-13" @default.
• W2056561441 title "A rapid and efficient determination of natural estrogens in soils by pressurised liquid extraction and gas chromatography–mass spectrometry" @default.
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• W2056561441 doi "https://doi.org/10.1016/j.chemosphere.2007.11.062" @default.
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