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• W2056564486 abstract "The synthesis of chiral periodic mesoporous organosilicas (ChiMO) of MCM-41 type using a bis-silylated tartramide derived from l-(+)-dimethyl tartrate (Sharpless and Kagan ligand) has been studied. The ChiMO materials were characterized by powder XRD, TEM, and nitrogen adsorption–desorption measurements, verifying their successful preparation. The evidence of the covalent bonding between the organic chiral precursor and the inorganic silica framework structure was confirmed by 13C and 29Si NMR solid state measurements. The synthesized chiral PMO was found to catalyze the asymmetric oxidation of thioanisole with good sulfoxide yield and moderate enantioselectivity. Reutilization of the “solid” chiral ligand led to similar optical yields to that obtained with the fresh ChiMO, revealing the true heterogeneous nature of the immobilized tartrate derivative." @default.
• W2056564486 created "2016-06-24" @default.
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• W2056564486 date "2008-04-10" @default.
• W2056564486 modified "2023-10-14" @default.
• W2056564486 title "Synthesis of Chiral Periodic Mesoporous Silicas Incorporating Tartrate Derivatives in the Framework and Their Use in Asymmetric Sulfoxidation" @default.
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• W2056564486 doi "https://doi.org/10.1021/cm703050u" @default.
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