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- W2056572748 abstract "The temperature dependence of the 1H spin-lattice relaxation time, T1, and of the second moment of 1H NMR spectra were studied in a series of trimethylammonium hexahalometallates(IV), (triMA)2MX6, (M = Pt, Sn, Te; X = Cl, Br, I). From X-ray powder diagrams taken at room temperature, it was found that these complexes are isomorphous throughout the series. The unit cell dimensions were determined. A single 35Cl NQR line was observed for (triMA)2SnCl6 and for (triMA)2TeCl6 in agreement with the crystal symmetry of these complexes. By 1H NMR, two kinds of motions of the ion (triMA), a) the intraionic reorientations of the CH3 groups and b) the reorientation of the whole cation about its C3 axis, have been observed separately in most of the complexes studied. The activation energies of these motions imply that the ions (triMA) are more freely rotating in the hexahalometallate(IV) complexes as compared to the (triMA) halides." @default.
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- W2056572748 date "1982-07-01" @default.
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- W2056572748 title "Molecular Motion of [(CH3)3NH]⊕ Ions in Solid Trimethylammonium Hexahalometallates(IV) as Studied by 1H NMR and 35Cl NQR" @default.
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- W2056572748 doi "https://doi.org/10.1002/bbpc.19820860722" @default.
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