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- W2056573560 abstract "The solid-state 13C n.m.r. spectrum of calcium D-xylo-5-hexulosonate, which exists exclusively in the β-furanose form, resembles that of the minor furanose form in solution. A 1H two-dimensional nuclear Overhauser enhancement spectrum (NOESY), however, unambiguously shows that the latter component is the α-furanose form. Thus caution is required in comparing liquid- and solid-state n.m.r. spectra. Longitudinal relaxation-rate measurements show that GdIII binds preferentially to the keto tautomer, in a bidentate fashion via a carboxylate oxygen and O(2). The first co-ordination sphere of GdIII in the predominant complex is completed by furanose ligands bound in a bidentate manner via the two carboxylate oxygens." @default.
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- W2056573560 date "1990-01-01" @default.
- W2056573560 modified "2023-09-30" @default.
- W2056573560 title "The structure of D-xylo-5-hexulosonic acid and its gadolinium(III) complexes in aqueous medium as studied by nuclear magnetic resonance" @default.
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- W2056573560 doi "https://doi.org/10.1039/dt9900002707" @default.
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