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- W2056596208 abstract "Two model systems consisting of (1) phenylurea herbicides and (2) nitro aromatics were chosen to demonstrate the potential of on-line trace enrichment. The liquid chromatography—mass spectrometry system consists of a 2-MM-I.D. precolumn and analytical column combined with a direct liquid-inlet interface with a helium jet principle. The mass spectrometer has been operated in the positive and negative chemical-ionisation modes. For the investigated compounds, on-line trace enrichment can give enrichment factors of two to three orders of magnitude. For dinitroaromatics detection limits of 0.01 parts per billion were obtained, which corresponds to absolute detection limits of 1 pg. Band broadening was of the order of 1 sec (σt)." @default.
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- W2056596208 date "1985-04-01" @default.
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- W2056596208 title "On-line trace enrichment for improved sensitivity in liquid chromatography with direct liquid introduction mass spectrometric detection" @default.
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- W2056596208 doi "https://doi.org/10.1016/s0021-9673(01)90375-9" @default.
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