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- W2056685412 abstract "Abstract The recovery of titanium from the slurry formed in crude titanium tetrachloride and recycling of NaCl–AlCl 3 was studied. Experimental results showed that the titanium contained in the slurry can be effectively recovered by reactive distillation with molten NaCl–AlCl 3 . More than 99% of titanium was volatilized from the slurry by distilling at 453 K for 40 min with slurry to molten salt (S/M) ratio of 1.8:1. Experiments found that the recovered titanium includes the chloride and oxychloride as the TiOCl 2 containing in the slurry was changed into TiCl 4 by the complex reactions of TiOCl 2 with AlCl 3 and NaAlCl 4 during reactive distillation. The behavior of molten NaCl–AlCl 3 during vacuum distillation was studied and NaCl–AlCl 3 was recovered from the reactive distillation residue (RD residue) by vacuum distillation. The study showed that high temperature and vacuum were favorable to the evaporation of NaCl–AlCl 3 . Meanwhile, 97.8% of AlCl 3 and 66.8% of NaCl were recovered from RD residue as distillate. The distillate was a mixture of AlCl 3 and NaAlCl 4 , which can be returned to reactive distillation by adding a small amount of NaCl." @default.
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- W2056685412 date "2014-10-01" @default.
- W2056685412 modified "2023-09-24" @default.
- W2056685412 title "Recovery of titanium from the slurry formed in crude TiCl4 by reactive distillation with NaCl–AlCl3 and recycling of NaCl–AlCl3 by vacuum distillation" @default.
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- W2056685412 doi "https://doi.org/10.1016/j.vacuum.2014.05.001" @default.
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