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• W2056792372 abstract "[3-11C]Phenylalanine has been prepared by a five-step synthesis beginning with 11CO2. [11C]Benzyl chloride was prepared by addition of11CO2 to phenylmagnesium bromide, hydride reduction to [11C]benzyl alcohol, and chlorination (CCl4, tri-n-octylphosphine). The [11C]benzyl chloride was then used to alkylate the anion of N-diphenylmethylene)glycine ethyl ester using phase-transfer catalysis. The protecting groups were removed by acidic hydrolysis to yield DL-[3-11C]phenylalanine in 25–31% overall radiochemical yield (decay corrected) in a synthesis time of 60–70 min." @default.
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• W2056792372 date "1984-07-01" @default.
• W2056792372 modified "2023-10-12" @default.
• W2056792372 title "Synthesis of DL-[3-11C]phenylalanine" @default.
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• W2056792372 doi "https://doi.org/10.1016/0020-708x(84)90103-0" @default.
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