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- W2056817940 abstract "The compounds [(CH3)4N]2MGe4S10(M= Fe, Cd, Mn, (Co, Mn)) have been synthesized under hydrothermal conditions in glass ampoules at 393 K for two days. They have been investigated by means of thermogravimetry, ionic chromatography, X-ray methods, and IR spectroscopy. They crystallize in the tetragonal symmetry, space groupI4. They are isostructural with [(CH3)4N]2MnGe4S10and their structures were refined from X-ray powder diffraction intensity data down to the final reliability factorsRF= 0.07 (RBragg= 0.08) andRF= 0.05 (RBragg= 0.05) for the Fe and Cd compounds, respectively. The structure consists of tetrahedra sharing apices with a space filling of the covalent (Ge,M)–S framework as small as 45%. The anionic framework generates tunnels with a diameter of about 7 Å, determined from structural results, running along the [100], [010], and [112] directions in which theTMAcations are located." @default.
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- W2056817940 date "1996-02-01" @default.
- W2056817940 modified "2023-10-09" @default.
- W2056817940 title "Structure Refinement by the Rietveld Method of the Thiogermanates [(CH3)4N]2MGe4S10(M= Fe, Cd)" @default.
- W2056817940 doi "https://doi.org/10.1006/jssc.1996.0065" @default.
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