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• W2057053028 startingPage "1025" @default.
• W2057053028 abstract "An analytical method for trace levels of iron in a seawater sample using isotope dilution ICP-MS was developed. Preconcentration of iron and the removal of major elements in seawater such as alkali and alkaline-earth elements can be carried out quickly using a chelating resin disk by adjusting the sample pH to 3. The collision cell option of the ICP-MS instrument method was used to improve the performance of the instrument for iron measurements since ArO and ArN interferences could be reduced using this analytical method. About 4 ml min(-1) helium, as the collision gas, were introduced into the cell. 40Ar14N and 40Ar16O which interfere with 54Fe and 56Fe in water had their amounts decreased by 5 orders of magnitude. Then, the isotope dilution method was used for iron determination below ng g(-1) level of trace iron in four environmental reference materials (river water standard sample JAC-0031 (Japan Soc. for Analytical Chemistry), estuarine standard sample SLEW-2 (NRC Canada) and seawater standard samples CASS-3 and NASS-5 (NRC Canada)) were measured. Good agreement between analytical results and certified values of reference materials was obtained, which confirmed the effectiveness of this method." @default.
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• W2057053028 date "2004-07-01" @default.
• W2057053028 modified "2023-09-24" @default.
• W2057053028 title "Determination of Trace Levels of Iron in a Seawater Sample Using Isotope Dilution/Inductively Coupled Plasma Mass Spectrometry" @default.
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• W2057053028 doi "https://doi.org/10.2116/analsci.20.1025" @default.
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