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- W2057148862 abstract "A range of spinels containing nickel, chromium and iron have been prepared by forming solid solutions of the appropriate single oxides at 950°C, in atmospheres of CO2 or CO2/2% CO. For each spinel series prepared a calibration curve has been generated which relates lattice parameter, as determined by X-ray diffraction, to spinel composition. These calibration curves facilitate the identification of the spinels in oxide layers formed on stainless steels. Energy dispersive X-ray analysis has been carried out on each standard spinel prepared to determine elemental composition. It was found that variations in the oxidizing or reducing nature of the reaction atmosphere affected the stability of spinels containing Fe(II) or Fe(III). Small quantities of nickel metal were identified in nickel rich spinels formed in CO2/CO atmospheres. This observation could be an important factor in the deposition behaviour of such surfaces under reactor conditions." @default.
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- W2057148862 date "1988-08-01" @default.
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- W2057148862 title "Characterization of nickel-chromium-iron spinel-type oxides" @default.
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- W2057148862 doi "https://doi.org/10.1016/0022-3115(88)90159-6" @default.
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