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• W2057166654 abstract "With specific annealing schemes applied to a neat polystyrene-block-poly(ethylene oxide) (SE) and its composites with cadmium sulfide quantum dots (CdS QD), we have observed microdomain structures and phase transitions in the system using temperature-resolved small-angle X-ray scattering (SAXS) and transmission electron microscopy (TEM). Both TEM images and SAXS results show clearly that incorporation of surfactant-tethered CdS QD preferentially into PEO blocks leads to increases in thermal stabilities of both bcc-packed lattice (referred as long-range order) and microdomains themselves in the sphere-forming SE/CdS composites. The bcc-packed lattice in the SE/CdS composites sustains better than that in the neat SE, during a temperature elevation to ∼160 °C, at which the bcc-packed SE/CdS spheres start to transform into micelles with a short-range liquid-like order. Quantitative model analysis shows that the PEO/CdS micelles can retain their size in the SE/CdS composites up to 200 °C, whereas the PEO micelles shrink after the softening of the PS matrix around 100 °C, and disassociate largely into the PS matrix of the neat SE at 160 °C." @default.
• W2057166654 created "2016-06-24" @default.
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• W2057166654 date "2006-02-01" @default.
• W2057166654 modified "2023-10-16" @default.
• W2057166654 title "Transitions of domain ordering and domain size in a spherical-forming polystyrene-block-poly(ethylene oxide) copolymer and its composites with colloidal cadmium sulfide quantum dots" @default.
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• W2057166654 doi "https://doi.org/10.1016/j.polymer.2005.12.055" @default.
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