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• W2057171036 endingPage "8221" @default.
• W2057171036 startingPage "8213" @default.
• W2057171036 abstract "We have carried out a mechanistic investigation of aerobic dehydrogenation of cyclohexanones and cyclohexenones to phenols with a Pd(TFA)2/2-dimethylaminopyridine catalyst system. Numerous experimental methods, including kinetic studies, filtration tests, Hg poisoning experiments, transmission electron microscopy, and dynamic light scattering, provide compelling evidence that the initial Pd(II) catalyst mediates the first dehydrogenation of cyclohexanone to cyclohexenone, after which it evolves into soluble Pd nanoparticles that retain catalytic activity. This nanoparticle formation and stabilization is facilitated by each of the components in the catalytic reaction, including the ligand, TsOH, DMSO, substrate, and cyclohexenone intermediate." @default.
• W2057171036 created "2016-06-24" @default.
• W2057171036 creator A5032981628 @default.
• W2057171036 creator A5042472739 @default.
• W2057171036 creator A5074617275 @default.
• W2057171036 date "2013-05-24" @default.
• W2057171036 modified "2023-10-16" @default.
• W2057171036 title "Aerobic Dehydrogenation of Cyclohexanone to Phenol Catalyzed by Pd(TFA)₂/2-Dimethylaminopyridine: Evidence for the Role of Pd Nanoparticles" @default.
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• W2057171036 doi "https://doi.org/10.1021/ja403165u" @default.
• W2057171036 hasPubMedCentralId "https://www.ncbi.nlm.nih.gov/pmc/articles/3796041" @default.
• W2057171036 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/23662607" @default.
• W2057171036 hasPublicationYear "2013" @default.
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